منابع مشابه
synthesis of sulfides from alcohols and thiols in solvent-freeconditions and deoxygenation of sulfoxides
کاتالیست یک سنتز جدید برای تیواترها توصیف شده است. واکنش الکل ها با آریل، هتروآریل و آلکیل تیو ل ها درحضور 1،3،5- تری آزو- 2،4،6- تری فسفرین-2،2،4،4،6،6 هگزاکلراید ((tapc به عنوان یک کاتالیست موُثر، بازده های خوب تا عالی از تیواترها را حاصل می کند. علاوه براین، واکنش تحت شرایط بدون فلز و بدون حلال پیش می رود، بنابراین یک مکمل جالب برای روش های شناخته شده سنتز تیواترها ارائه می دهد. یک مکانیسم ا...
15 صفحه اولLipase Mediated Isoamyl Acetate Synthesis in Solvent-Free System Using Vinyl Acetate as Acyl Donor
Synthesis of isoamyl acetate, a flavour ester extensively used in food industry, has been carried out in a solvent-free system. In the present study, an attempt has been made to enhance the isoamyl acetate synthesis yield by transesterification of isoamyl alcohol with vinyl acetate using immobilized Rhizopus oryzae NRRL 3562 lipase. In the present synthesis, substrates had no inhibitory effect ...
متن کاملAn Expeditious One-pot Synthesis of Imidazo[1,2-a]pyridines using ZnCl2.SiO2 as a Recyclable Heterogeneous Catalyst under Solvent-free Condition
Synthesis of imidazo[1,2-a]pyridines over several solid supported catalysts has been investigated. Among these catalysts, ZnCl2 .SiO2 (silzic) showed excellent yields and short reaction times. The silzic catalyst could be recovered and reused in five reaction cycles. The present procedure offers several advantages such as short reaction time, simplicity of the reaction procedure, the eliminatio...
متن کاملSynthesis and Characterization of 2,6-Dihydroxy Substituted Chalcones Using PEG-400 as a Recyclable Solvent M.R.Jayapal, K.Sreenivasa Prasad, and N.Y.Sreedhar
A novel method for the synthesis of 2,6-dihydroxy substituted chalcones via Claisen-Schmidt is introduced using recyclable PEG-400 as an alternative reaction solvent. The reaction is clean with excellent yield, shorter reaction time and reduces the use of volatile organic compounds (VOCs). The structures of the synthesized compounds were confirmed by IR, mass spectroscopy and elemental analysis.
متن کاملSynthesis of Thiazole Derivatives via Multicomponent Reaction of Tetramethyl thiourea using Water as a Safe Solvent
An efficient synthesis of 1,3-thiazole drivatives is described via a three component reaction isothiocyanates, tetramethyl thiourea and ethyl bromopyruvate.
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ژورنال
عنوان ژورنال: Arkivoc
سال: 2011
ISSN: 1551-7012
DOI: 10.3998/ark.5550190.0012.222